Silicone Resin
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Complete Bubble Removal for Silicone! Defoaming Test of Potting & Sealing Materials
日期:2026-09-11作者:小施Full Bubble Elimination for Silicone! Defoaming Field Test for Potting & Sealing
Solve bubble issues in silicone potting, sealing and thermal pads, covering low-viscosity LSR to high-viscosity pastes
Silicone is an elastic polymer based on polydimethylsiloxane (PDMS). It features outstanding high & low temperature resistance (-60℃~250℃), electrical insulation, hydrophobicity and biological inertness. Classified by curing mechanism into addition-curable (platinum-catalyzed) and condensation-curable types. Widely used in electronic potting, LED encapsulation, thermal interface materials (TIM), building sealing, medical devices, cosmetics and personal care products. Air is easily entrapped during silicone stirring, filler dispersion and dispensing. Some systems feature ultra-high viscosity and strong thixotropy. Residual bubbles may trigger poor insulation, decreased thermal conductivity, sealing failure and surface defects. SIENOX delivers efficient defoaming solutions for various silicone materials via self-developed planetary mixing & defoaming technology.
◆ Material Properties
Matrix Type Addition-curable (platinum catalyst), Condensation-curable (tin-catalyzed / oxime-type / alcohol-type) | Filler System Fumed silica, thermally conductive alumina / boron nitride, calcium carbonate, color pigment | Viscosity Range 500~500,000+ cps, from free-flowing liquid to high-viscosity paste |
Mixing Ratio One-component RTV / two-component 1:1~10:1 / LSR injection molding | Curing Condition Room temp curing / heating 100-150℃ / high temp vulcanization 170-200℃ | Defoaming Challenges High-filled thermal silicone with strong thixotropy; platinum-catalyzed systems highly sensitive to air bubbles |
◆ Mature Application Fields
🔌 Electronic Potting Potting protection for power modules, LED drivers, sensors, connectors and other electronic components (viscosity 1,000~15,000cps) | 💡 LED Encapsulation Encapsulation lens for LED chips/strips/modules, requiring high transmittance and resistance to high-temperature yellowing (low-viscosity high-transparency system) | 🔥 Thermal Interface Materials Thermal silicone pads, thermal conductive gels, thermal gap fillers (high-filled alumina/boron nitride, viscosity 50,000~300,000cps) |
🏗️ Building Sealing Curtain wall structural adhesive, door & window sealant, stone bonding adhesive, insulating glass sealing (high-viscosity high-thixotropy system) | 🏥 Medical / Daily Chemical Medical-grade silicone tubes, catheters, nipples, cosmetic injection fillers, defoaming for cosmetic formulations | 🔋 New Energy Battery Thermal pads for battery modules, battery pack sealing & potting, three-proof coating for BMS circuit boards (flame-retardant thermal conductive system) |
🎨 Crafts / Molds Silicone mold reproduction, silicone molds for resin/candle/soap, food-grade silicone products (low & medium viscosity system) | 🚗 Automotive Sealing Lamp sealing, windshield bonding, engine gasket forming, wire harness waterproof sealing (oil & weather resistant system) | ⚡ PV Modules Potting for PV junction boxes, terminal sealing, module frame sealing (weather-resistant & anti-UV system, 25-year service life requirement) |
◆ Core Problems Caused by Bubbles
⚡ Degraded Insulation / Thermal Performance Internal bubbles create thermal resistance / electrical weak points. Thermal conductivity drops by 30-50%, breakdown voltage decreases significantly and heat dissipation deteriorates | 🔘 Surface Defects & Sealing Failure Burst surface bubbles form pinholes and pits. Risk of leakage on sealing interface increases, failing waterproof & moisture-proof requirements |
🧪 Abnormal Curing Bubbles hinder full contact of A/B components, resulting in incomplete local curing, tackiness, soft spots and uneven rebound | 💡 Deteriorated Optical Performance Bubbles scatter light in LED encapsulation lenses and optical-grade silicone, reducing transmittance, causing uneven light spots and lower luminous efficiency |
◆ Recommended Process — Planetary Mixing & Defoaming
Step 1 Material Preparation Weigh silicone base material and curing agent/crosslinker according to ratio. Ensure accurate proportion of A/B for two-component systems; preheat high-viscosity materials to 40-60℃ to reduce viscosity | Step 2 Vacuum Mixing & Defoaming Put mixture into mixing cup, set vacuum at -95KPa and planetary mixing parameters. The machine completes mixing and vacuum defoaming synchronously in one cycle |
Step 3 Dispensing / Pouring Dispense or pour immediately after defoaming. Pour slowly along container wall to avoid re-entrapped air; finish operation within pot life | Step 4 Curing & Forming Cure under specified temperature & duration. For addition-curable silicone, avoid platinum catalyst poisoning from sulfur or phosphorus-containing materials |
◆ Recommended Equipment
MIX60 — Capacity 5~60g, suitable for lab R&D and small batch potting sample defoaming; excellent effect for low-viscosity silicone (500~10,000cps)
MIX90 — Capacity 20~500g, suitable for medium-batch production and medium-viscosity thermal silicone (10,000~80,000cps) defoaming; uniform planetary mixing
MIX1000PLUS — Capacity 100~1,000g, suitable for mass production and defoaming of high-viscosity high-filled thermal gel / sealant (80,000~300,000+ cps)
MIX2000 — Capacity 500~2,000g, suitable for industrial continuous production and batch defoaming of large potting parts
◆ Test Cases
▶ Case 1: Low-viscosity Electronic Potting Silicone Defoaming
Test Material | Two-component addition-curable silicone potting compound (for LED driver power supply potting, A/B=1:1, transparent free-flowing liquid) |
Initial Viscosity | 3,000 cps (25℃) |
Test Model | MIX60 |
Vacuum Level | -95 KPa |
Rotation Speed | 1,500 rpm |
Defoaming Time | 3 min |
Material Temp. | 25℃ (Ambient) |
✅ Defoaming Result: Mixing + defoaming finished in 3 minutes. No visible bubbles on cross-section of potting part, transmittance>95%, Shore A hardness 25 after curing, breakdown voltage>20KV/mm, meeting potting requirements for LED driver power supplies.
▶ Case 2: Medium-viscosity Thermal Silicone Defoaming
Test Material | Thermal conductive silicone gel (for CPU/GPU heat dissipation, high-filled alumina thermal powder, A/B=1:1, grey paste) |
Initial Viscosity | 35,000 cps (25℃) |
Test Model | MIX90 |
Vacuum Level | -95 KPa |
Rotation Speed | 2,000 rpm |
Defoaming Time | 5 min |
Material Temp. | 40℃ (preheat for viscosity reduction) |
✅ Defoaming Result: Mixing + defoaming finished in 5 minutes. Cross-section porosity of thermal gel<1%, thermal conductivity stable at 3.5 W/m·K, interfacial thermal resistance reduced by 40%, meeting requirements for consumer electronics heat dissipation modules.
▶ Case 3: High-viscosity Building Sealant Defoaming
Test Material | One-component dealcoholized silicone building sealant (curtain wall structural adhesive, high-thixotropy paste, with calcium carbonate reinforcing filler) |
Initial Viscosity | 150,000 cps (25℃) |
Test Model | MIX1000PLUS |
Vacuum Level | -95 KPa |
Rotation Speed | 2,500 rpm |
Defoaming Time | 8 min |
Material Temp. | 50℃ (preheat for viscosity reduction) |
✅ Defoaming Result: Mixing + defoaming finished in 8 minutes. Sealant extrudes continuously without bubble breakage, smooth surface free of pinholes, elongation at break>400%, no cracking after weathering test (1000h UV aging), meeting standards for building curtain wall sealing.
◆ Before & After Comparison
Comparison Item | Before Defoaming | After Defoaming |
Internal Density | Cross-section porosity 5-15%, uneven distribution | Cross-section porosity<1%, uniform & dense structure |
Thermal Conductivity | Bubbles cause thermal insulation, low & fluctuating measured values | Stable thermal conductivity, interfacial thermal resistance reduced by 40% |
Curing Integrity | Local tackiness & soft spots, uneven curing | Fully & evenly cured, consistent hardness/elasticity data |
Sealing & Waterproof Performance | Bubble channels cause leakage, IP rating failure | Complete sealing interface, stable IP67 protection rating |
Transmittance (Optical Parts) | Light scattered by bubbles, hazy & whitening | Transmittance>95%, optically clear & uniform |
Yield Rate | High rework rate, poor batch consistency | Yield>99%, stable & controllable batches |
🎯 Free Sample Testing
Send your silicone samples to us. We will test defoaming parameters and issue test reports.